文章信息/Info

Title:

 FIB three-dimensional characterization analysis techniques and its application progress

作者:

賈志宏; 王雪麗; 邢遠(yuǎn); 劉瑩瑩; 劉慶

(重慶大學(xué)材料科學(xué)與工程學(xué)院，重慶400044）

Author(s):

 JIA Zhihong;  WANG Xueli;  XING Yuan;  LIU Yingying;  LIU Qing

 (College of Materials Science and Engineering，Chongqing University，Chongqing 400044，China)

關(guān)鍵詞:

 ; FIB三維表征技術(shù); 3D-SIMS; 3D-Imaging; 3D-EDX; 3D-EBSD

DOI:

10.7502/j.issn.1674-3962.2013.12.04

文獻(xiàn)標(biāo)志碼:

A

摘要:

 聚焦離子束（Focused ion beam, FIB）技術(shù)憑借其獨(dú)特的微納尺度制造能力和優(yōu)勢(shì)，已成為納米科技工作者不可或缺的工具之一。隨著新型FIB硬件設(shè)備的多功能化，F(xiàn)IB三維表征技術(shù)的不斷完善，使FIB三維表征技術(shù)在材料研究領(lǐng)域的應(yīng)用更加廣泛和深入。與其他三維表征技術(shù)相比,FIB三維表征技術(shù)具有控制精度高、分析微觀區(qū)域大、分辨率高等特點(diǎn)。FIB技術(shù)與SIMS、SEM、EDX、EBSD等系統(tǒng)的結(jié)合，可對(duì)不同材料進(jìn)行三維空間狀態(tài)下的形貌、成分、取向等信息的分析。本文簡(jiǎn)要概述了3D-SIMS、3D-Imaging/EDX、3D-EBSD四種基于FIB的三維表征技術(shù)，具體包括FIB三維表征技術(shù)的成像-切割的原理及過程，綜述了幾種不同表征手段在各種材料中的應(yīng)用和發(fā)展，最后指出了FIB三維表征技術(shù)在應(yīng)用中的一些不足以及對(duì)該技術(shù)發(fā)展方向的展望。

Abstract:

 Focused ion beam(FIB) technology has become one of indispensable tool in nano technology area with its unique micro-Nano-scale manufacturing capability and advantages. With multi-functionalizing of the new type hardware and improving of the 3D characterization technology, the applications of FIB 3D characterization technology in the field of materials research became more extensive and in-depth. FIB 3D characterization technology has many distinctive features, compared to other 3D characterization technology, such as highly controllable accuracy, largely detectable region, high resolution and so on. FIB technology can analysis the morphology, composition, orientation of different materials in three-dimensional space conditions when it combined with SIMS, SEM, EDX or EBSD systems. This paper briefly summarized four different 3D characterization technologies include 3D-SIMS, 3D-Imaging/EDX and 3D-EBSD, and introduced the details of imaging-cutting principle and process of FIB 3D characterization technology. At the same time, this paper also summarized the applications and the development of several different characterization methods in different materials, and pointed out some deficiencies in application and prospects for the development direction of the FIB 3D characterization technology in the end.